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2020 Vol.32, Issue 3 Preview Page

Research Article

Validation of Analytical Method of Pectolinarin for Standardized Cirsium setidens Fine Powder by Air-Classification

공기분급을 이용한 곤드레 미세분말의 Pectolinarin성분 분석법 검증

S. J. Park1†
,
H. D. Kim2
,
Y. H. Lee3
박 성진1†
,
김 현덕2
,
이 윤환3
1Professor, Department of Tourism Food Service Cuisine, Hallym Polytechnic University
2Director, Channuri Life Co. Ltd.
3CEO, Channuri Life Co. Ltd.
1한림성심대학교 관광외식조리과 교수
2(주)찬누리라이프 이사
3(주)찬누리라이프 대표이사
*sjpark@hsc.ac.kr
31 December 2020. pp. 407-416
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Abstract

This study aimed to validate the determination of pectolinarin from standardized Cirsium setidens fine powder by air classification. High-performance liquid chromatography was used to measure specificity, linearity, precision, accuracy, limit of detection (LOD), and limit of quantification (LOQ). From the calibration curve, we obtained a correlation coefficient of 0.9979 for pectolinarin. The inter-day and intra-day precision values of pectolinarin ranged from 0.28% to 2.35%. The inter-day and intra-day accuracies were 90.20－115.62% and 90.63.113.05%, respectively. The LOD and LOQ for pectolinarin were 0.11.µg/mL and 0.34. µg/mL, respectively. Therefore, the analytical method was validated for the detection of pectolinarin from air-classified Cirsium setidens fine powder.

Keywords
Cirsium setidens
Air-classification
Fine powder
HPLC method
Validation
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Information
  • Publisher :Agriculture and Life Sciences Research Institute, Kangwon National University
  • Publisher(Ko) :None
  • Journal Title :Journal of Agricultural, Life and Environmental Sciences
  • Volume : 32
  • No :3
  • Pages :407-416
  • Received Date : 2020-10-21
  • Revised Date : 2020-12-08
  • Accepted Date : 2020-12-10
  • DOI :https://doi.org/10.22698/jales.20200035
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